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The Laser Gold Story

(Shown at Right)
The product that changed the direction of Epner Technology's future; the fusing reflector for the Xerox Model 3100 copier. This aluminum extrusion was polished, nickel and gold plated, eventually on the functional surfaces only, and became the beta site product for our future infrared plating experience. More than a million were produced at Epner.

Our first experience exhibiting at a trade show was in 1972. The Design Engineering Show at McCormick Place in Chicago. A draftsman from Xerox stopped at our booth and admired all the gold plated stuff and an aluminum part caught his eye. He said Xerox was having a problem with adhesion of nickel and gold at 500F. The part was the fusing reflector for a new line of copiers and this part was the "gating" item for the program.

I left the booth in the hands of a colleague and flew directly to Rochester to meet with the engineer whose name he had given me.
The Xerox engineers gave me an extruded aluminum sample to plate. The spec was: Polish (buff) the reflecting surfaces, Bright nickel plate followed by a bright, pure gold, 0.25 microns thick.

I returned a week later and proudly presented the part. I was ushered into a darkened room with four engineers. They mounted the extrusion in a holder on the side of a machine I had never seen before but the marking read, Beckman DK 2A.. This I learned was a spectrophotometer with an integrating sphere and thus could measure the total reflective efficiency. Specular combined with diffuse. They were measuring at a wavelength of 700 nm. and the reflectivity came up on the digital readout at 94%.

Their jaws dropped. They tried not to look impressed, but they failed. I too, could hardly hide my excitement at their excitement even though I didn't know what I was looking at.

The sent me back to NY with 20 more samples but I could have flown without a plane. Two weeks later, we repeated the routine. Only this time the reflectivity barely reached 91%!The lead engineer freaked. He said, " I put you on the drawing at 91% to give you a 3% cushion. Now I've got to drop it to 88%" What happened to the 94%?"

I tap-danced. I didn't know how we got 94% in the first place, but of course I assured him that we would maintain the 91% and surely would get back to the higher reflectivity as "soon as our lab figured it out". But the parts didn't blister in the heat test so we were off and running with a 500 piece pre production order.
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We delivered the first production parts of some of the most beautiful gold plating we had ever done. They were all rejected. Low reflectivity! It was evident that the human eye made a very poor IR spectrophotometer. Indeed, in the infrared, gold is not gold, is not gold.

It was immediately clear that if we didn't have the same measuring instrument that Xerox used, the game was over. They agreed and tooled us with the identical set up.. With the new "eyes" that our in-house Beckman gave us, we were able, over some two years of production, to get back to 94% at 700nm. Today we guarantee 97% at 700nm! And recently, that aging DK2A, was joined by a Perkin-Elmer Lambda 9. Of course with an integrating sphere. (We picked up Am-Ray Scanning Electron Microscope at that same auction) see Quality Stuff.

Infrared Spectrophotometer With Intergrating Sphere

Perkin-Elmer Lambda 750 Infrared Spectrophotometer with intergrating sphere.

With its integrating sphere attachment, the DK2A is the heart of Laser Gold quality maintenance. It measures total infrared reflectivity (i.e. specular and diffuse) in the range of from 700nm to 2500nm and is calibrated to the NIST Standard 2011, supplied by Epner to the then, NBS, for more than fifteen years.

 

Epilogue: All the while we sought higher and higher reflectivity, Xerox engineering was pushing us to make the gold harder. Paper exiting the copier would eventually wear away the coating. By the end of the program some ten years later, we were plating a pure gold that was also hard! (200 Knoop)! This break through permitted us to cut the gold thickness in half, with no degradation in life of the part.

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How Did a Small Company in Brooklyn Become a Supplier to NIST of The Infrared Reflectance Standard?

Curiously, it is another story that involves Xerox.. We were shipping reflectors for fusing the toner on one of the best selling copiers that Xerox had ever built. Thousands a week. Remember, this was in the 70's when Xerox owned the copier business.

Their QC department rejected a shipment for low reflectivity which we knew met the spec. After all, we were calibrating our Beckman Spectrophotometer with an NBS (National Bureau of Standards) as NIST was then known, and they were using a standard that their optics lab manager had produced. Our NBS Standard was a quartz flat with a vapor deposited gold on one surface.

I flew to Xerox in Rochester NY with my NBS standard in hand for the “shoot out.” Frank Winski, the manager of the optics lab, no trivial position at Xerox, measured the NBS mirror on his Beckman, the identical instrument to ours incidentally, and actually told me, “The NBS standard is 2% off”. I said, “Frank, that’s like saying there is no God. Your calibration must be off.” To my great annoyance, he refused to back down. The reject would stand.

I called the NBS Metrology group in Gaithersburg, MD., and made an appointment for the next day. They remeasured their mirror and to their dismay (and mine), indeed agreed that the vapor deposited gold had degraded with time.

It was not a pleasant scene. I assumed a recall of all the outstanding IR Standards was being discussed, but as “the messenger” I was not eager to hang around. When I thought a sufficient amount of time had passed, I send a Laser Gold coated mirror for their consideration as an IR Standard. It was measured and put aside.

When it was remeasured a year later and exhibited the theoretically high reflectivity of gold and the ability to be physically cleaned, they ordered 50 mirrors. These were aged for five years and finally offered to the optics industry, unchanged from the day we shipped them. Proud of our achievement, Cohan Epner, as the company was then called, ordered the first Laser Gold coated IR Standard.

NIST continued

 

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