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Brooklyn, NY A superplastic
fabricating process, patented by McDonnell Douglas Corp.,
now (Boeing) heats a sheet of titanium to its superplastic
temperature directly inside the forming press; no furnace
is necessary. Energy from the heat source, a bank of 1600W
infrared (IR) lamps, is directed to the metal via a water-cooled,
gold-plated reflector. Pressurized argon gas forces the sheet
into the die.
An electrodeposited gold, developed by Epner
Technology Incorporated, makes this possible by providing
a better than 98% reflector efficiency. Called Laser
Gold (the material is the industry standard coating
for pump cavity reflectors of Nd:Yag solid-state lasers),
the coating permits repeated physical cleaning with no apparent
wear or degradation of reflectivity.
Problem:
Used by the McDonnell Douglas St. Louis facility to fabricate
parts for the F-15 Eagle and the F-18 Hornet aircraft, the
superplastic forming process (SPF) originally employed a polished
aluminum reflector. High temperatures, however, promoted oxidation.
The reflector, consequently, was disassembled on a monthly
basis, repolished, and then reassembled. Polishing compound
inadvertently left on the reflector surface stimulated even
faster oxidation.
At best, the aluminum surface reflected
only 75 to 80% of the incident IR energy. To boost efficiency,
the company considered conventional gold plating. Coatings
produced by vapor deposition offered the desired reflectivity
(95 to 98%) but wiped away with successive cleanings. Ordinary
electroplating produced a hard coat, but the relatively small
increase in reflectivity (approximately 10%) did not justify
the added expense.
Solution:
Laser Gold combines the high reflectivity of vapor
deposition with the durability of electroplating. Impervious
to high temperatures generated by the IR lamps, the coating
eliminates oxidation. No oxidation, in turn, eliminates disassembly
and repolishing. Occasional lamp removal for surface cleaning
constitutes the only required maintenance.
Plating begins by polishing the aluminum
reflector to an RMS 4 finish. Degreasing and an aluminum preplate
preparation using the zincate process follow. Since aluminum
cannot be directly plated with gold, an electroless nickel
plating precedes gold deposition.
The nickel, deposited to a minimum thickness
of 0.001 inch, acts as a barrier between the aluminum and
gold, preventing the gold from diffusing into the aluminum.
It also provides a better bond for gold plating. Once deposited,
the nickel plate is buffed and electrochemically activated
prior to gold plating.
Electrodeposition of a gold layer measuring
at least 100 uinches in thickness, makes up the last step.
Although electroplating traditionally calls for direct current,
Epner Technology Incorporated superimposes ac on the dc. Repeated
pulses of electricity and trace amounts of proprietary additives,
product the coatings unique crystalline structure. The
structure, different from that formed by conventional electroplating,
gives the gold near optimum reflectivity at IR wavelengths
between 2 and 5 microns.
Another factor contributing to the coatings
overall performance involves, when applicable, a plating/deplating
procedure. The company plates the substrate metal for several
seconds, reverses polarity, and deplates for a
shorter interval. The cycle is then repeated several times.
The entire process took more than 15 years to develop.
Additional
benefits, applications:
Besides bringing the titanium sheet to its superplastic temperature,
the high-power, IR lamps preheat the female die the
large mass of steel below the titanium sheet. Since the Laser
Gold reflector absorbs less than 2% of the energy striking
it, more energy is directed at the die. This translates to
significant decreases in cycle times and/or power reductions
ranging up to 50%.
The electrodeposition process applies not
only to aluminum, but to a variety of substrates. These include
molybdenum, beryllium, magnesium and titanium. When a vacuum
deposited binder coating is applied to dielectric materials,
they too can be electroplated with gold. IR missiles; countermeasure
systems designed to protect aircraft (including Air Force
One and the Space Shuttle vehicles) from IR homing missiles;
and use in IR ovens for industrial purposes (e.g., curing
rubber, drying paint, etc.) represent current applications.
Additional details
Contact Epner Technology
Incorporated, 25 Division Place, Brooklyn, NY 11222, 718-782-5948
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Epner's Laser Gold
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